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Journal Articles Progress in Nuclear Magnetic Resonance Spectroscopy Year : 2021

Practical dissolution dynamic nuclear polarization

Stuart Elliott
  • Function : Author
Quentin Stern
  • Function : Author
Morgan Ceillier
  • Function : Author
Théo El Daraï
  • Function : Author
Samuel Cousin
  • Function : Author
Olivier Cala
  • Function : Author


This review article intends to provide insightful advice for dissolution-dynamic nuclear polarization in the form of a practical handbook. The goal is to aid research groups to effectively perform such experiments in their own laboratories. Previous review articles on this subject have covered a large number of useful topics including instrumentation, experimentation, theory, etc. The topics to be addressed here will include tips for sample preparation and for checking sample health; a checklist to correctly diagnose system faults and perform general maintenance; the necessary mechanical requirements regarding sample dissolution; and aids for accurate, fast and reliable polarization quantification. Herein, the challenges and limitations of each stage of a typical dissolutiondynamic nuclear polarization experiment are presented, with the focus being on how to quickly and simply overcome some of the limitations often encountered in the laboratory.
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Dates and versions

hal-03954523 , version 1 (24-01-2023)



Stuart Elliott, Quentin Stern, Morgan Ceillier, Théo El Daraï, Samuel Cousin, et al.. Practical dissolution dynamic nuclear polarization. Progress in Nuclear Magnetic Resonance Spectroscopy, 2021, 126-127, pp.59-100. ⟨10.1016/j.pnmrs.2021.04.002⟩. ⟨hal-03954523⟩
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